Laboratory of MicroAnalysis
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N.N. Vorozhtsov Novosibirsk Institute of Organic Chemistry
 of Siberian Branch of Russian Academy of Sciences

Tikhova_V_D

Head - Cand. of Chemical Sciences  Vera Dmitrievna Tikhova

phone +7 (383) 330-98-56
internal phone: 3-33
email:This email address is being protected from spambots. You need JavaScript enabled to view it.

 

Short history

Short history:


Microanalytical Laboratory is one of the few laboratories among existing today, which was organized in the early years of the Novosibirsk Institute of Organic Chemistry.

Nikolai Nikolayevich Vorozhtsov, the first Director of the Institute, was well aware that the work relating to the synthesis of organic compounds, and the allocation of natural substances, can not develop without the analytical data. Therefore, in 1959 two female employees of the Institute were entrusted with establishing methods for determining the carbon, hydrogen and nitrogen in organic matter. And in beginning of 1960 “the analytical laboratory” was established with that title until 1967.

Lyudmila Nikolayevna Diakur began to work at the Institute as the head of this laboratory and directed it until her retirement in 1974. With extensive experience in analytical chemistry, as well as having organizational skills, L.N.Diakur has done much to selecting laboratory personnel and to developing required methods of analysis. In the first years classical methods were established for the determination of carbon, hydrogen, nitrogen, halogens, sulfur, and some of the functional groups (alkoxy, acetyl, active hydrogen, etc). In 1967 automatic CHN-analyzer (Hewlett-Packard) and vapor phase osmometer (for determining molecular weight) were purchased for the laboratory. The appearance of CHN-analyzer stimulated studies on the effective oxide catalysts for determining the elements with this device.

In 1975 Valentina Pavlovna Fadeeva became the head of the laboratory. Intensive development of synthetic works in the Institute, particularly in the field of chemistry polyfluoroaromatic, heterocyclic compounds required the development of methods for analysing these compounds. So much time in the laboratory was devoted to developing methods for determining fluorine and other elements in polyfluoroaromatic substances. In the 70th years thermoanalytical method appeared in the lab.It should be noted that our Director Academician N.N.Vorozhtsov always been very attentive to our lab, watching our progress, and help, when necessary. We began to publish scientific papers, organized city seminar on the organic analysis in Novosibirsk. Our laboratory was well equipped and had a good methodological support, thus became known among analysts from the Urals to the Far East. Some analysts from Irkutsk, Tomsk, Krasnoyarsk, Barnaul, Novokuznetsk, Sverdlovsk and other cities come to our laboratory for training.

In 1980, the group of gas chromatography entered into the laboratory, with whom we had been working for almost 20 years. This group has developed the universal methods of analysing polyfluoroaromatic and substituted aromatic compounds, which are now used for routine analysis. In 80’s the laboratory began to analyse working area air, and in the early 90's - the wastewater of the Institute. The results of our research are reported on a variety of analytical conferences, we have been involved in organizing the conference "Analytica of Siberia and the Far East," printed papers in national and international journals. Laboratory carries out tests for many organizations, first and foremost, for the Institutes of SB RAS.Students of NSU and other universities, students of the Novosibirsk Mendeleev Chemical Engineering College do their theses and course works in the laboratory.

The laboratory had been accredited three times since 1995, now it prepares for the next accreditation, that confirms the competence of the laboratory in the field of analysising organic compounds. All developed laboratory techniques for elemental analysis are metrologically certified and entered in the Federal Register of Analytical Techniques. Now our equipment is considerably upgraded, we have new CHNO-and CHNS-analyzers, vapor phase osmometer, termoanalyzer, modern UV-VIS spectrophotometers.

Our laboratory still maintains its status and prestige among analysts. We would like to preserve this tradition. Our work is usually “behind the scenes”. We should always be in the "alert" to run smoothly and with good quality. Not everyone can safely handle such a monotonous and painstaking work, as we have. It requires concentration, attentiveness, neatness. These qualities, as well as a favorable atmosphere are the main secret of our successful work.


Determining the elemental composition of synthetic and natural compounds and materials of various composition and structure by organic elemental analysis and atomic emission spectroscopy; designing and upgrading the analytical procedures. Determining the molecular weight of organic compounds and osmolality of solutions by vapor phase osmometry. Analysis of waste water and workplace air to detect toxic elements and compounds.



Research areas:

Research areas:


  • Determining the elemental composition of synthetic and natural compounds and materials of various composition and structure by organic elemental analysis and atomic emission spectroscopy; designing and upgrading the analytical procedures.
  • Determining the molecular weight of organic compounds and osmolality of solutions by vapor phase osmometry.
  • Analysis of waste water and workplace air to detect toxic elements and compounds.
 

The Laboratory carries out the determination of the following elements by using both instrumental and chemical methods: carbon, hydrogen, nitrogen, sulfur, phosphorus, halogens (chlorine, bromine, iodine, fluorine), selenium, oxygen.

The Laboratory has the following advanced equipment:


  • automatic CHNS and CHNO elemental analyzers EURO EA;
  • vapor phase osmometer KNAUER K-7000;
  • thermal analyzer STA 409 PC Luxx NETZSCH;
  • UV-VIS spectrophotometers Cary 50 and Cary 60 VARIAN;
  • Set of balances with different weighing range and sensitivity METTLER and SARTORIUS;
  • Conductometer ANION;
  • Thermosystem METTLER for determination of melting point.

The main research results in recent years


  • The universal oxide catalyst compositions was developed to provide a complete decomposition of various substances and the absorption of interfering elements when determining the carbon, hydrogen, nitrogen, sulfur in automatic analyzers, as well as in the classical method of determining the C and H.
  • The method of determining fluorine was developed, including the oxidative degradation of the sample in an oxygen atmosphere, followed by spectrophotometry (for complex-alizarinkomplekson lanthanum fluoride) or potentiometry (with a fluoride-selective electrode), the presence of another halogens, sulfur, phosphorus, metals in analyzed substances does not interfere fluorine determination; the method allows to determine fluorine content when present in the sample to 80%.
  • The technique of sulfur determination was developed using potentiometric titration with barium-selective electrode.
  • The method of selenium determination in organoselenium materials, based on the combustion of a substance in a flask filled with oxygen, and then determining the resulting Se (IV) extraction-spectrophotometric reaction with aromatic diamines-new reagent 3,4,5,6-tetrafluoro-1 .2-diaminobenzene and the previously known 2.3-diaminonaftalin. The presence of halogens and sulfur in analyzed substances, does not interfere selenium determination.
  • The fragment composition of different origin soil and peat humic acids was investigated using a computer system "IR EXPERT”.
  • Proposed methods has been successfully applied for analyzing virtually any substance, including hard degradable substances, such as a fully fluorinated, not containing hydrogen, including graphite, sulfur, halogen-, phosphorus-containing aromatic, polycyclic, heterocyclic nitrogen, metallic (complex, intercalation, organometallic, etc.), carbon materials, such as coal, sapropel, bitumens and their products, polymers, industrial oils, petroleum, rocks, etc.
  • The vapor phase osmometry is used to determine the molecular weight poorly volatile organic and natural substances.
  • Thermoanalytical method is applied for determining the thermal characteristics of the material and the thermal decomposition reaction kinetics. The thermal stability of substituted naphthoquinones, some polyfluoroaromatic compounds, sterically hindered phenols - stabilizers of polymeric materials was investigated.
  • The mechanisms of the thermal decomposition of some compounds were suggested. The new software "TERMOGRAF" was developed for the calculation of kinetic parameters of thermolysis.
 

We are constantly working to improve the methods of analyzing organic compounds and to increase the number of elements determined.

Our studies were supported by the integration project of the Siberian Branch of the Russian Academy of Sciences and held in conjunction with the Institute of Soil and Agrochemistry SB RAS and the Institute of Petroleum Chemistry SB RAS (Tomsk).
The employees of laboratory take part in national and international conferences. The laboratory is preparing for accreditation as part of the Testing Analytical Center IOC SB RAS. The Laboratory constantly analyzes various substances and objects for other organizations of SB RAS: International Tomography Center, Institute of Catalysis, Institute of Inorganic Chemistry, Institute of Soil and Agrochemistry, Institute of Kinetics and Combustion, Institute of Chemical Biology and Fundamental Medicine, etc.


List of priority investigations

  • 2008-2012
    • 5.4 "Chemical aspects of modern ecology and environmental management, including the scientific problems of recycling and safe storage of radioactive waste".
    • Program V.39.2 «Development of physical and chemical principles of safety of human activities" Green Chemistry ".
    • Project V.39.2.5«Development of the research methodology of low molecular weight organic compounds and materials, reactions and processes in living systems using a new highly informative spectroanalytical methods".
  • 2013-2016 the laboratory will work on priority:
    • V 46. "Physico-chemical basis of environmental management and environmental protection on the basis of the principles of" green chemistry "and high catalytic systems to create new resources and energy saving steel and chemical processes, including the deep processing of hydrocarbon mineral resources of different classes and industrial waste, as well as new technology for processing of spent nuclear fuel and radioactive waste".
    • Program V.36.1. "Development of physical and chemical principles and methods of environmental protection and recycling of industrial waste on the basis of the principles of" green chemistry "and catalytic systems".
    • Inter-laboratory research project - "Development of an integrative studies of organic matter and synthetic materials, natural and anthropogenic, reactions and processes in living systems and environmental samples".
 
 
 
STAFF:

Staff

№ Employee Position Room Phone Phone in. email Publications
by years
1 Tikhova Vera Dmitrievna Lab's Head (Cand. Chem) 411 НТК, 125 330-65-54, 330-98-56 2-39, 3-33 This email address is being protected from spambots. You need JavaScript enabled to view it.
2 Lastovka Anastasiya Valerievna Researcher (Cand. Chem.) 126 330-65-54 3-73 This email address is being protected from spambots. You need JavaScript enabled to view it.
3 Deryabina Yulia Mikhailovna Leading Engineer 111 330-65-54 4-20 This email address is being protected from spambots. You need JavaScript enabled to view it.
4 Nikulicheva Olga Nikolaevna Leading Engineer 126 330-65-54 3-73 This email address is being protected from spambots. You need JavaScript enabled to view it.
5 Dobrinskaya Tatyana Alekseevna technicist 123 330-65-54 4-04
6 Lazareva Nadezhda Viktorovna technicist 123 330-65-54 4-04
7 Usova Olga Viktorovna technicist 123 330-65-54 4-04
8 Bender Chrisina Nikolaevna laboratory assistant
9 Shabelnikova Anna Mikhailovna laboratory assistant
10 Lisina Tatiana Victorovna Senior Laboratory Assistant
Students
11 Titova Anastasiya Sergeevna laboratory assistant
PHD Students
12 Zubricheva Darya Vladislavovna Junior Researcher 126 330-65-54 3-73
13 Petrakova Svetlana Yur'evna Junior Researcher 126 This email address is being protected from spambots. You need JavaScript enabled to view it.


PUBLICATIONS
 

Publications over the past years

Laboratory staff publications (DB NIOCh)

Reviews, Articles


2022
  1. DETERMINATION OF FLUORINE IN ORGANIC FUNCTIONAL MATERIALS/ Tikhova V.D., Fadeeva V.P., Nikulicheva O.N., Dobinskaya T.A., Deryabina Yu.M.// Chemistry for Sustainable Development. 2022. Т. 30. № 6. С. 640-653. doi:10.15372/CSD2022427
  2. PHYSICOCHEMICAL INVESTIGATION OF HOMESPUN CULT OBJECTS OF THE KHANTY AND MANSI MADE AT THE END OF THE XVIII CENTURY/ Karpova E.V., Sotnikova Yu.S., Lastovka A.V., Baulo A.V., Salnikova I.V.// Chemistry for Sustainable Development. 2022. Т. 30. № 6. С. 585-594. doi:10.15372/CSD2022421
  3. A. Kotlyarova, A.V. Podturkina, A.V. Pavlova, D.S. Gorina, A.V. Lastovka, O.V. Ardashov, A.D. Rogachev, A.E. Izyurov, A.B. Arefieva, A.V. Kulikov, T.G. Tolstikova, K.P. Volcho, N.F. Salakhutdinov, Yu. Sidorova
    A Newly Identified Monoterpenoid-Based Small Molecule Able to Support the Survival of Primary Cultured Dopamine Neurons and Alleviate MPTP-Induced Toxicity In Vivo
    Molecules 2022, 27(23), 8286; doi:10.3390/molecules27238286, IF=4.927
  4. D.V. Zubricheva, A.V. Lastovka, I.V. Il'ina, K.P. Volcho, V.D. Tikhova, V.P. Fadeeva, N.F. Salakhutdinov
    Determination of elemental impurities Cd, Pb, As, Hg, Co, V, Ni, Pd, Ru, Ag, Pt, Mo, Al, and Fe in highly potent analgesic activity agent by microwave-induced plasma optical emission spectrometry (MIP OES)
    Chemical Papers, 2020, V. 76, N 9, Pp. 5677-5689 doi:10.1007/s11696-022-02275-0, IF=2.146
  5. A.A. Bogush, G.A. Leonova, S.K. Krivonogov, V.A. Bychinsky, V.A. Bobrov, A.E. Maltsev, V.D. Tikhova, L.V. Miroshnichenko, L.M. Kondratyeva, A.E. Kuzmina
    Biogeochemistry and element speciation in sapropel from freshwater Lake Dukhovoe (East Baikal region, Russia)
    Applied Geochemistry, 2022, V. 143,105384 doi:10.1016/j.apgeochem.2022.105384, IF=3.841
  6. S.N. Bizyaev, Yu.V. Gatilov, D.V. Zubricheva, V.D. Tikhova, A.V. Tkachev
    A New Type of Terpene-Based D 2-Symmetric Macrocycles, Capable of Selectively Extracting Au, Pd and Pt from Complex Mixtures
    ChemistrySelect, V.7, N 22, June 13, 2022, e202201263 doi:10.1002/slct.202201263, IF=2.307

2021
  1. T. Skripkina, M. Belokozenko, S. Shatskaya, V. Tikhova, I. Lomovskiy
    Concentrating rare earth elements in brown coal humic acids by mechanochemical treatment Check for updates
    RSC Advances, 2021, V. 11, N 57, Pp 36016-36022 doi:10.1039/D1RA07228E, IF=3.361
  2. ELEMENTAL COMPOSITION OF BROWN COAL, BITUMEN AND HUMIC ACIDS MOTORISCHE FIELD KHMAO-YUGRY/ GUROVA O.A., SARTAKOV M.P., ANANYINA I.V., COLORED D.I., DERYABINA YU.M//

2020
  1. A.A. Bogush, C. Dabu, V.D. Tikhova, J.K. Kim, L.C. Campos
    Biomass Ashes for Acid Mine Drainage Remediation
    Waste and Biomass Valorization, 2020, V. 11, N 7, Pp 4977-4989 doi:10.1007/s12649-019-00804-9, IF=2.851
  2. S.G. Mamylov, T.S. Skripkina, V.D. Tikhova, A.L. Bychkov, O.I. Lomovsky
    Thermal analysis of mechanochemically activated humic acids of brown coal
    Journal of Physics: Conference Series 1675 (2020) 012093 doi:10.1088/1742-6596/1675/1/012093
  3. V.A. Logvinenko, V.P. Fadeeva, B.A. Selivanov, V.D. Tikhova, A.A. Nefedov, A.Ya. Tikhonov
    Thermal decomposition of several N,N'-bis(2-hydroxyiminoalkyl)-α,α'-dinitrones
    Journal of Thermal Analysis and Calorimetry, 2020, V. 140, N 2, Pp 685-693 doi:10.1007/s10973-019-08868-4, IF=2.731
  4. G.N. Chekhova, D.V. Pinakov, Yu.V. Shubin, V.P. Fadeeva, V.D. Tikhova, A.V. Okotrub, L.G. Bulusheva
    Room temperature synthesis of fluorinated graphite intercalation compounds with low fluorine loading of host matrix
    Journal of Fluorine Chemistry, 2020, V. 232, 109482 doi:10.1016/j.jfluchem.2020.109482, IF=2.332
  5. Analytical Control of Impurities and Active Components in (-)-Isopulegol Derivative - Highly Potent Analgesic Agent/ Lastovka A.V, Fadeeva V.P., Il'ina I.V., Salakhutdinov N.F.// Pharmaceutical Chemistry Journal doi:10.1007/s11094-020-02176-0, IF=0.538

2019
  1. A. V.Lastovka,A. D.Rogachev,I. V.Il'ina,A.Kabir,K.P.Volcho,V. P.Fadeeva,A.G.Pokrovsky,N. F.Salakhutdinov,K. G.Furtonc
    Comparison of dried matrix spots and fabric phase sorptive extraction methods for quantitation of highly potent analgesic activity agent (2R,4aR,7R,8aR)-4,7-dimethyl-2-(thiophen-2-yl)octahydro-2H-chromen-4-ol in rat whole blood and plasma using LC–MS/MS
    Journal of Chromatography B, 2019, V. 1132, Art. Number 121813 doi:10.1016/j.jchromb.2019.121813, IF=2.789
  2. V.D. Tikhova, Yu.M. Deryabina, R.S. Vasilevich, E.D. Lodygin
    Structural features of tundra and taiga soil humic acids according to IR EXPERT analytical system data
    Journal of Soils and Sediments, 2019, V. 19, N 6, pp 2697-2707 doi:10.1007/s11368-018-2097-x, IF=2.669
  3. Zinc(II) Complexes with Tetrafluoroterephthalic and Octafluorobiphenyl-4,4'-dicarboxylic Acid Anions and 1,10-Phenanthroline/ S. V. Larionov, M. I. Rakhmanova, L. A. Glinskaya, D. Yu. Naumov, A. S. Vinogradov, V. M. Karpov, V. E. Platonov, V. P. Fadeeva// Russian Journal of General Chemistry, 2019, V. 89, N 2, pp 261-265 doi:10.1134/S1070363219020154, IF=0.643

2018
  1. Mechanochemical Solid-Phase Reactions of Humic Acids from Brown Coal with Sodium Percarbonate/ T. S. Skripkina, A. L. Bychkov, V. D. Tikhova, O. I. Lomovsky// Solid Fuel Chemistry, 2018, V. 52, IN 6, pp 356-360 doi:10.3103/S0361521918060101, IF=0.553
  2. А.В. Ластовка, Е.Ю. Яковлева, В.Ф. Коллегов, В.П. Фадеева, Н.Ф. Салахутдинов
    Определение остаточных органических растворителей методом газовой хроматографии в субстанции (2R,4R,4AR,7R, 8AR)-4,7-диметил-2-(тиофен-2-ил)октагидро-2H-хромен-4-ол, обладающей анальгетической активностью
    Заводская лаборатория. Диагностика материалов. 2018. Т. 84. № 9. С. 13-20. doi:10.26896/1028-6861-2018-84-9-13-20
  3. T. Skripkina, A. Bychkov, V. Tikhova, B. Smolyakov, O. Lomovsky
    Mechanochemically oxidized brown coal and the effect of its application in polluted water
    Environmental Technology & Innovation, 2018, V. 11, Pp 74-82 doi:10.1016/j.eti.2018.04.010
  4. А.П. Крысин, В.П. Фадеева, О.Н. Никуличева, А.А. Нефедов
    Решение алгоритма: фенольные антиоксиданты - путь к улучшению механических свойств полимерных материалов
    Химия в интересах устойчивого развития. 2018. Т. 26. № 2. С. 149-155 doi:10.15372/KhUR20180205

2017
  1. A.V. Lastovka, V.P. Fadeeva, M.A. Bazhenov, V.D. Tikhova
    Rapid Determination of Tellurium in Tellurium-Containing Organic Compounds by Microwave Plasma - Atomic Emission Spectrometry
    Orient J Chem 2017;33(6), pp 2796-2802 doi:10.13005/ojc/330612
  2. A.L. Bychkov, Al.I. Denkin, V.D. Tikhova, O.I. Lomovsky
    Prediction of higher heating values of plant biomass from ultimate analysis data
    Journal of Thermal Analysis and Calorimetry, , 2017, V. 130, N 3, pp 1399-1405 doi:10.1007/s10973-017-6350-0, IF=1.952
  3. M.P. Sartakov, N.V. Shpynova, I.D. Komissarov, Yu.M. Deryabina
    The Elemental Composition of Humic Acids of Sapropels: A Study for Lakes of the Upper and Middle Priobye, West Siberia
    International Journal of Ecology & Development, 2017, V. 32, N4 , Pp 138-144
  4. А. В. Ластовка, В. П. Фадеева, И. В. Ильина, С. Ю. Курбакова, К. П. Волчо, Н. Ф. Салахутдинов
    Исследование физико-химических свойств и разработка методики определения (2R,4R,4aR,7R,8aR)-4,7-диметил-2- (тиофен-2-ил)октагидро-2H-хромен-4-ола, обладающего высокой анальгетической активностью
    Заводская лаборатория, 2017, Т. 83, № 10, С. 11-17 doi:10.26896/1028-6861-2017-83-11-17
  5. Yu.M. Deryabina, T.A. Kornakova, N.L. Bazhina, V.D. Tikhova
    Comparative Infrared Spectra Analysis of One Territory Soil Humic Acids by IR-EXPERT Computer System
    IInt. J. Green. Pharm. 2017 (Suppl); 11(3), pp S465-S469 (http://greenpharmacy.info/index.php/ijgp/article/view/1158) doi:10.22377/ijgp.v11i03.1158
  6. О.В. Федотова, И.В. Грехова, Ю.М. Дерябина, В.Д. Тихова
    Сравнительный анализ фракций при производстве гуминового препарата росток
    Аграрный вестник Урала, 2017, № 5 (159), С. 12.

2016
  1. А.А. Bogush, V.G. Voronin, V.D. Tikhova, G.N. Anoshin
    Acid Rock Drainage Remediation and Element Removal Using a Peat-Humic Agent with Subsequent Thermal Treatment of the Metal-Organic Residue.
    Mine Water and the Environment Journal, December 2016, V. 35, N 4, pp 536-546 doi:10.1007/s10230-015-0380-2, IF=0.864
  2. Synthesis and photoluminescence of Eu(III) complex compounds containing anions of perfluoro-3-methylbenzoic acid/ S. V. Larionov, M. I. Rakhmanova, V. M. Karpov, V. E. Platonov, V. P. Fadeeva// Russian Journal of General Chemistry, December 2016, Volume 86, Issue 12, pp 2677-2681 doi:10.1134/S1070363216120173, IF=0.481
  3. Determination of Boron in Organic Compounds by Microwave Plasma-Atomic Emission Spectrometry/ M.A. Bazhenov, V.D. Tikhova, V.P. Fadeeva// Journal of Analytical Chemistry, 2016, Vol. 71, No. 11, pp. 1089-1095. doi:10.1134/S1061934816090033, IF=0.694
  4. E.M. Osnitsky, M.P. Sartakov, E.A. Zarov, Yu.M. Deryabina
    Elemental Composition of the Humic Acids in the High-Moor Peats of the Western Siberia Taiga Zone.
    Research Journal of Pharmaceutical, Biological and Chemical Sciences. 2016. V. 7. N 6. Pp. 3104-3113
  5. The research of electronic spectrum absorbtion of peats’ humic acids of Western Siberia middle Taiga Zone/ M.P. Sartakov, I.D. Komissarov, Yu.M. Deryabina// Вестник Красноярского государственного аграрного университета. 2016. № 7 (118). С. 48-55.
  6. M.P. Sartakov, Y.M. Deryabina, N. Komissarov
    Elemental analysis of humic acids in peat resources of Khantymansiysk Autonomous region - Ygra
    International Journal of Pharmacy and Technology, 2016, V. 8, N 2, Pp 14244-14255
  7. M.P. Sartakov, E.D. Lapshina, E.M. Osnitsky, E.A. Zarov, Yu.M. Deryabina
    The Thermal Stability Comparative Analysis of Humic Acids in the Sphagnous Peat of the Western Siberia Taiga Zone Raised Bogs.
    Research Journal of Pharmaceutical, Biological and Chemical Sciences. 2016. V. 7. N 5. Pp. 1311-1320
  8. G.A. Selivanova, E.V. Tretyakov, E.V. Amosov, I.Yu. Bagryanskaya, V.G. Vasiliev, E.V. Vasilyev, V.D. Tikhova, E.V. Karpova, T.V. Basova, D.V. Stass, V.D. Shteingarts
    X-Ray induced phase transitions in 4-((4-(dibutylamino)phenyl)diazenyl)-biphenyl-2,3',4'-tricarbonitrile
    Journal of Molecular Structure, V. 1107, 5 March 2016, Pp 242-248 doi:10.1016/j.molstruc.2015.11.060, IF=1.779
  9. T.F. Mikhailovskaya, A.G. Makarov, N.Yu. Selikhova, A.Yu. Makarov, E.A. Pritchina, I.Yu. Bagryanskaya, E.V. Vorontsova, I.D. Ivanov, V.D. Tikhova, N.P. Gritsan, Y.G. Slizhov, A.V. Zibarev
    Carbocyclic functionalization of quinoxalines, their chalcogen congeners 2,1,3-benzothia/selenadiazoles, and related 1,2-diaminobenzenes based on nucleophilic substitution of fluorine
    Journal of Fluorine Chemistry, V. 183, March 2016, Pp 44-58 doi:10.1016/j.jfluchem.2016.01.009, IF=2.213

2015
  1. M.P. Sartakov, Y.M. Deryabina, N.V. Chuhareva
    Thermodynamical stability and element composition peat humic acids Khanty-Mansiysk district
    Research Journal of Pharmaceutical, Biological and Chemical Sciences, 2015, V. 6, N 5, Pp 1589-1593
  2. Elemental Composition of Humic Acids in Sapropel of the Middle Ob Region and the South of the Ob-Irtysh Basin in West Siberia/ SARTAKOV M.P., SHPYNOVA N.V., DERYABINA YU. M., KOMISSAROV I.D.// Chemistry for Sustainable Development, 2015. №5. С.523-526 doi:10.15372/KhUR20150503
  3. Фадеева В.П., Дерябина Ю.М., Никуличева О.Н., Тихова В.Д.
    Одновременное определение галогенов в органических соединениях с использованием ионоселективных электродов
    Заводская лаборатория. Диагностика материалов. 2015. Т. 81. № 7. С. 19-23.
  4. С.В. Ларионов, Л.И. Мячина, Л.А. Шелудякова, И.В. Корольков, М.И. Рахманова, П.Е. Плюснин, А.С. Виноградов, В.М. Карпов, В.Е. Платонов, В.П. Фадеева
    Синтез октафторбифенил-4,4'-дикарбоновой кислоты и фотолюминесцирующих соединений на ее основе
    Журнал общей химии. 2015. Т. 85. № 7. С. 1092-1098., IF=0.477
  5. M. Sartakov, Y. Deryabina, I. Komissarov
    Thermodynamic stability and chemical composition of humic acids of peat of the Khanty-Mansi area
    Proceedings of the XIV International Academic Congress " Fundamental and Applied Studies in the Modern World "(United Kingdom, Oxford, 23-25 May 2015) . “Oxford University Press”, 2015.
  6. A comparative analysis of humic acids from Khakassia paleosols using ir-expert computer program/ Tikhova V.D., Bogdanova T.F., Dergacheva M.I., Fadeeva V.P., Kallas E.V.// Теоретическая и прикладная экология. 2015. № 1. С. 24-27.

2014
  1. Determination of organogenic elements in the composition of functional compounds and materials/ V. P. Fadeeva, V. D. Tikhova, Yu. M. Deryabina, O. N. Nikulicheva// Journal of Structural Chemistry, September 2014, V. 55, N 5, pp 972-979 doi:10.1134/S0022476614050278, IF=0.5
  2. Specificity light absorption in visible and ultraviolet regions of humic acids of soils western part of the territory Tuva/ Bazhina N.L., Ondar E.E., Deryabina Y.M.//
  3. А.Л. Бычков, А.И. Денькин, В.Д. Тихова, О.И. Ломовский
    Расчет теплоты сгорания лигноцеллюлозы на основании данных элементного анализа
    Химия растительного сырья, 2014, N 3, C. 99-104
  4. Preparation of photoluminescent compounds of Eu(III), Sm(III), and Dy(III) containing anions of tetrafluoroterephthalic acid/ S. V. Larionov, L. I. Myachina, L. A. Sheludyakova, I. V. Korol’kov, O. V. Antonova, V. M. Karpov, V. E. Platonov, V. P. Fadeeva// Russian Journal of General Chemistry, 2014, V. 84, N 6, pp 1193-1197. doi:10.1134/S107036321406022X, IF=0.418
  5. Extraction-spectrophotometric determination of selenium in organoselenium compounds using aromatic o-diamines/ V.P. Fadeeva, D.O. Panin, O.N. Nikulicheva, V.D. TikhovaВ. П. Фадеева, Д. О. Панин, О. Н. Никуличева, В. Д. Тихова// Journal of Analytical Chemistry, May 2014, V. 69, N 5, pp 432-437. doi:10.1134/S1061934814030034, IF=0.811
  6. О.В. Рыбачук, Ю.М. Дерябина, М.П. Сартаков, И.Д. Комиссаров
    Сравнительная характеристика элементного состава гуминовых и гиматомелановых кислот торфов Среднего Приобья.
    Аграрная наука Евро-Северо-Востока, 2014, №1(38), С.36-40.

2013
  1. Н.В. Чухарева, В.Д. Тихова, О.Н. Зарубина, Л.В. Шишмина
    Изменение элементного состава и оптических свойств торфа под действием термической модификации
    Вестник Красноярского ГАУ, 2013, N 11, С.85-94.
  2. В.Г. Меркулов, Д.В. Кабанов, В.Н. Митькин, И.А. Сукачева, В.П. Фадеева
    Исследование металлоносности фракций углеродистого вещества, выделенных флотацией из руд и технологических материалов Зун-Холбинского черносланцевого золоторудного месторождения, с применением ИНАА и других методов анализа. 1. Поведение матричных сидерофильных и халькофильных элементов при флотации
    Известия ВУЗов. Физика, 2013, Т. 56, N 11-3, С.238-242., IF=0.407
  3. A Thermoanalytic Method for the Analysis of Biologically Active Substances using Isobornylphenol Derivatives as an Example/ O. N. Nikulicheva, A. P. Krysin, V. P. Fadeeva, E. A. Krasnov, E. E. Nazmutdinova// Pharmaceutical Chemistry Journal, 2014, V. 47, N 11, pp 616-619. doi:10.1007/s11094-014-1021-y, IF=0.319
  4. A.A. Bogush, G.A. Leonova, S.K. Krivonogov, V.A. Bobrov, V.D. Tikhova, L.M. Kondratyeva, A.E. Kuzmina, A.E. Maltsev
    Diagenetic transformation of sapropel from Lake Dukhovoe (East Baikal region, Russia)
    Procedia Earth and Planetary Science, 7(2013), P.81–84. doi:10.1016/j.proeps.2013.03.161
  5. Synthesis and photoluminescence of Eu(III) and Tb(III) complex compounds containing anions of 4-CF3C6F4COOH and 4-(CF3)(2)CFC6F4COOH acids/ S. V. Larionov, T. G. Leonova, E. M. Uskov, M. I. Rakhmanova, V. E. Platonov, V. M. Karpov, V. P. Fadeeva// Russian Journal of General Chemistry, 2013, V. 83 N 6, Pp 1117-1122. doi:10.1134/S1070363213060194, IF=0.432
  6. Study of the fragment composition of humic acids of different origin using IR-EXPERT software/ V. D. Tikhova, T. F. Bogdanova, V. P. Fadeeva, V. N. Piottukh-Peletsky// Journal of Analytical Chemistry, 2013, V. 68, N 1, Pp 86-94. doi:10.1134/S1061934813010139, IF=0.615
  7. V.D. Tikhova, V.P. Fadeeva
    Chapter: Methodical Basis of Analysis for Various Genesis of Humic Acids
    in Functions of Natural Organic Matter in Changing Environment, 01/2013: pages 165-169; , ISBN: 978-94-007-5633-5

2012
  1. М.И. Дергачева, О.А. Некрасова, Д.И. Васильева, В.П. Фадеева
    Элементный состав гуминовых кислот целинных черноземов разных условий формирования
    Вестник Оренбургского государственного университета, 2012, № 12(146), 90-96.
  2. Syntheses and structures of p-HOOCC6F4COOH˙H2O (H2L ˙H2O) and luminescent coordination polymers [Tb2(H2O)4(L)3˙2H2O] n and Tb2(Phen)2(L)3˙2H2O/ S.V. Larionov, L.I. Myachina, L.A. Glinskaya, I.V. Korol'kov, E.M. Uskov, O.V. Antonova, V.M. Karpov, V.E. Platonov, V.P. Fadeeva// RUSS J COORD CHEM+, 2012, V. 38, N 12, pp. 717-723. doi:10.1134/S1070328412110036, IF=0.546

2011
  1. Synthesis and photoluminescence of Zinc(II) complexes with tetrafluoroterephthalic acid (H2L). Crystal structure of coordination polymer [Zn(H2O)4L•4H2О]n/ S.V. Larionov, L.I. Myachina, R.F. Klevtsova, L.A. Glinskaya, N.V. Kurat'Eva, E.M. Uskov, M.I. Rakhmanov, V.M. Karpov, V.E. Platonov, V.P. Fadeeva// RUSS J COORD CHEM+, 2011, V. 37, N 9, pp 650-656. doi:10.1134/S1070328411090041, IF=0.591

2010
  1. Composition determination of post-metallocene olefin polymerization catalysts/ Fadeeva V., Tikhova V., Nikulicheva O., Oleynik I.// J STRUCT CHEM+, 2010, V. 51, N 1 Supplement, p186 doi:10.1007/s10947-010-0211-z, IF=0.453

2009
  1. М.П.Сартаков, В.Д.Тихова
    Графостатистический анализ и спектроскопия ЯМР 13С молекул гуминовых кислот торфов среднего Приобья.
    Вестник КрасГАУ, N 6, 2009, с.76-80.
  2. М.П.Сартаков, В.Д.Тихова
    Термическая характеристика гуминовых кислот торфов среднего Приобья.
    Вестник КрасГАУ, N 11, 2009, с.26-29.
  3. Luminescence properties of complexes Ln(Phen)(C6F5COO)3 (Ln=Tb, Eu) and Ln(C6F5COO)5•nH2O (Ln=Tb, n=2; Ln=Eu, n=1). Structures of the Tb22(H2O)8(C6F5COO)6] complex and its isomer in the supramolecular compound [Tb2(H2O)8(C6F5COO)6]•2C6F5COOH/ S.V. Larionov, L.A. Glinskaya, T.G. Leonova, R.F. Klevtsova, E.M. Uskov, V.E. Platonov, V.M. Karpov, V.P. Fadeeva// Russian Journal of Coordination Chemistry, 2009, V. 35, N 11, pp 798-806. doi:10.1134/S1070328409110025, IF=0.533
  4. The effect of chemical modification on the chromatographic properties of polymeric adsorbents polysorb-1 and hisep Q and the diatomite carrier chromosorb P NAW/ E.Y. Yakovleva, V.Y. Belotserkovskaya, V.P. Fadeeva, G.S. Litvak, E.A. Paukshtis, D.E. Babushkin// Russian Journal of Physical Chemistry A, 2009, V . 83, N 5, pp. 849-853. doi:10.1134/S003602440905029X, IF=0.474

2008
  1. Elemental Analysis of Organic Compounds with the Use of Automated CHNS Analyzers/ V. P. Fadeeva, V. D. Tikhova, O. N. Nikulicheva// Journal of Analytical Chemistry, 2008, Т. 63, № 11, pp 1094-1106 doi:10.1134/S1061934808110142, IF=0.602
  2. Analysis of humic acids from various soils using acid hydrolysis/ V. D. Tikhova, V. P. Fadeeva, M. I. Dergacheva, M. M. Shakirov// Russian Journal of Applied Chemistry November 2008, Volume 81, Issue 11, pp 1957-1962 doi:10.1134/S1070427208110177, IF=0.268
  3. Kinetics of thermolysis of sterically hindered phenols used as polymeric material stabilizers/ O. N. Nikulicheva, A. P. Krysin, V. P. Fadeeva// Russian Journal of Applied Chemistry, 2008, V. 81, N 9, pp 1592-1596 doi:10.1134/S107042720809022X, IF=0.268
  4. Determination of sulfur in organic compounds using a barium-selective electrode/ V. P. Fadeeva, V. I. Vershinin, E. A. Kuzmina// Journal of Analytical Chemistry, 2008, Т. 63, № 8, С. 775-778. doi:10.1134/S106193480808011X, IF=0.602
  5. Silver(I) compounds with perfluorinated aromatic thiols C6F5C6F4SH, C10F7SH and C6F5SH as precursors for silver nanoparticles/ S.V. Larionov, T.G. Leonova, N.I. Batrachenko, I.V. Korol'kov, V.S. Danilovich, V.E. Platonov, A.M. Maksimov, V.P. Fadeeva// Russian Journal of Inorganic Chemistry, 2008, V. 53, N 2, Pp. 209-212. doi:10.1134/S0036023608020101, IF=0.589

2007
  1. Supramolecular structure of 6-phenyl-2-chloropyrimidine-4-carboxamide and its complexes with dioxane and ethanol/ T. V. Rybalova, V. P. Krivopalov, Yu. V. Gatilov, O. N. Nikulicheva, O. P. Shkurko// Journal of Structural Chemistry, 2007, V. 48, N 2, pp 318-324 doi:10.1007/s10947-007-0048-2, IF=0.344

2006
  1. Separation of pyrimidine derivatives by reversed-phase high-performance liquid chromatography/ V. P. Fadeeva, O. N. Nikulicheva, V. N. Kobrina// Russian Journal of Applied Chemistry, 2006, V. 79, N 12, pp 1994-1997 doi:10.1134/S1070427206120172, IF=0.18
  2. The structural characteristics and homogeneity regions of solid phases in the digraphite fluoride-acetonitrile system/ D. V. Pinakov, K. A. Khaldoyanidi, G. N. Chekhova, V. A. Logvinenko, Yu. V. Shubin, V. P. Fadeeva// Russian Journal of Physical Chemistry, t 2006, V. 80, N 8, pp 1198-1204 doi:10.1134/S0036024406080036, IF=0.25
  3. А.А. Иванов, Н.В. Юдина, О.И. Ломовский, В.Д. Тихова, В.П. Фадеева
    Механохимические превращения водорастворимых полисахаридов торфа
    Химия твердого топлива, 2006, № 6, 13-19.
  4. Interaction of heavy metal ions with ammonium humates/ A. D. Budaeva, E. V. Zoltoev, V. D. Tikhova, N. V. Bodoev// Russian Journal of Applied Chemistry, 2006, V. 79, N 6, pp 920-923 doi:10.1134/S1070427206060103, IF=0.18
  5. С.В. Ларионов, Т.Г. Леонова, Н.И. Батраченко, И.В. Корольков, Р.Ф. Клевцова, Л.А. Глинская, В.Е. Платонов, А.П. Крысин, А.М. Максимов, В.П. Фадеева
    Синтез и термические свойства соединений Pd(II) с перфторированными ароматическими тиолами и тиольным производным фенола
    Химия в интересах устойчивого развития, 2006, Т. 14, № 2, 147-154.

Selected publications


  1. V.P.Fadeeva, I.M.Moryakina. The use of different oxidation catalysts for the automatic determination of carbon, hydrogen and nitrogen in organic compounds.Izv. Sib. Otd. Akad. Nauk SSSR, Ser.: Khim., 1981, V.6, N.14, p 113.
  2. V.P.Fadeeva, I.M.Moryakina. Spectrophotometric determination of fluorine in fluorine-organic substances. Moscow, 1989; dep. in VINITI № 2579-889.
  3. O.N.Nikulicheva, V.P.Fadeeva and V.A.Logvinenko. Estimation of Thermal Stability of Phenol Stabilizers by Means of Thermogravimetric Analysis. J. Therm. Anal., 44, 329 (1995); Full text
  4. O.N.Nikulicheva, V.P.Fadeeva and V.A.Logvinenko. Calculation of the kinetic parameters thermal decomposition of some phenol stabilizers on the basis of thermoanalytical data. J. Therm. Anal., 47, 1629 (1996); Full text
  5. V.D.Tikhova, M.M.Shakirov, V.P.Fadeeva, M.I.Dergacheva. Specific Features of Humic Acids from Various Soils as Studied by Thermal Analysis and 13C NMR. Russian Journal of Applied Chemistry, 1998, N.7, p.1173.
  6. V.D.Tikhova, M.M.Shakirov, V.P.Fadeeva, M.I.Dergacheva. 31P NMR Study of Soil Humic Acids. Russian Journal of Applied Chemistry, 2000, N.7, p.1206.
  7. O.N. Nikulicheva, V.P.Fadeeva, V.N.Piottukh-Peletsky , L.M.Pokrovsky, T.F.Bogdanova, N.V.Yudina. An IR and GC-MS Study of Substances Extracted from Peat. Russian Journal of Applied Chemistry, 2005, V.78, N.8, p.1388.
  8. V.P.Fadeeva, V.D.Tikhova, O.N.Nikulicheva. Elemental analysis of organic compounds with the use of automated CHNS analyzers. Journal of Analytical Chemistry, 2008, V.63, N.11, p.1197.
  9. V.P.Fadeeva, V.D.Tikhova, O.N. Nikulicheva, I.V.Oleynik, I.I.Oleynik.Composition determination of post-metallocene olefin polymerization catalysts. Journal of Structural Chemistry, 2010, V.51, Supplement 1, p.188.
  10. V.D.Tikhova; T.F.Bogdanova, V.P.Fadeeva , V.N.Piottukh-Peletsky. Study of Fragment Composition of Humic Acid of Different Origin Using IR-EXPERT Software. Journal of Analytical Chemistry, 2013, V.68, N.1, p.86.
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